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Micro-mechanical evaluation of hard coatings

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Schiopetto Castro, Maria Florencia
Author's e-mailflor_mdq4arrobahotmail.com
Tutor / directorLlanes Pitarch, Luis MiguelMés informacióMés informacióMés informació; Jiménez Piqué, EmilioMés informacióMés informacióMés informació
Document typeMaster thesis
Date2020-07-06
Rights accessOpen Access
All rights reserved. This work is protected by the corresponding intellectual and industrial property rights. Without prejudice to any existing legal exemptions, reproduction, distribution, public communication or transformation of this work are prohibited without permission of the copyright holder
Abstract
Due to the continuous evolution of the industry, there has been an increasing demand for cutting tools that have properties such as significant hardness, resistance to corrosion, and wear. This has motivated the research, development and implementation of coatings that present a combination of good mechanical and tribological properties, which increase the performance of these tools. For this reason, throughout this work, the effect that monolayer (CrAlSiN) and multilayer (CrAlN) coatings have on micromechanical properties has been analyzed and compared. In addition, the effect of working with different bilayer thicknesses, and the effect of different types of substrates (Inconel, 1.2344 steel and WC-Co) have been analyzed. Scratch adhesion, monotonic spherical indentation, and microhardness tests were performed. The damages obtained after performing each test were evaluated through light microscopy, confocal microscopy and SEM. It was verified that when using multilayer coatings, an improvement in the micromechanical properties is obtained. And in turn, these properties improve with their bilayer thickness. In this way, an increase in hardness was obtained that was from 19% to 76% compared to the monolayer coating. In turn, an improvement in adhesion was obtained, as well as the contact pressure necessary for the appearance of plastic deformation. On the other hand, it was demotivated that among the three substrates analyzed, WC-Co is the one that presents a better combination of the analyzed properties. In this way, by having a monolayer coating on said substrate, even higher results are obtained, than when multilayer coatings are used on the steel. Lately, thanks to the tribological and mechanical properties of diamond coatings such as carbon (DLC), their use in industry has increased. That is why, the knowledge of the factors that control their properties and, therefore, the final performance of the coated components in practical tribological applications, becomes increasingly important. In this work, from the DLC samples analyzed, using the Ramana spectroscopy technique, two different structures were identified. Thus, one is known as amorphous carbon and the other is known as amorphous tetrahedral carbon. The latter is expected to present a better combination of mechanical properties.
SubjectsMaterials -- Mechanical properties, Coatings, Fracture mechanics, Materials -- Propietats mecàniques, Revestiments, Deformacions (Mecànica), Mecànica de fractura
DegreeMÀSTER UNIVERSITARI ERASMUS MUNDUS EN CIÈNCIA I ENGINYERIA DE MATERIALS AVANÇATS (Pla 2014)
URIhttp://hdl.handle.net/2117/336096
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  • Màsters oficials - European Master in Advanced Materials Science and Engineering - AMASE [61]
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