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Vitrification and devitrification during the non-isothermal cure of a thermoset. A TOPEM Study

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10.1007/s10973-009-0601-7
 
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hdl:2117/10298

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Fraga Rivas, Iria
Hutchinson, John M.Més informacióMés informació
Montserrat Ribas, SalvadorMés informació
Document typeArticle
Defense date2010-03
Rights accessRestricted access - publisher's policy
All rights reserved. This work is protected by the corresponding intellectual and industrial property rights. Without prejudice to any existing legal exemptions, reproduction, distribution, public communication or transformation of this work are prohibited without permission of the copyright holder
Abstract
The processes of vitrification and devitrification that occur in an epoxy resin when it cures nonisothermally with a hardener are studied in terms of their frequency dependence and as a function of the heating rate. A novel modulated DSC technique, TOPEM, has been used which permits the evaluation of the frequency dependence for a single sample in a scan at constant underlying heating rate, thus avoiding errors arising from the composition of the sample. The effects of both frequency and heating rate on vitrification and devitrification are investigated. Some advantages of this technique are observed and discussed.
CitationFraga, I.; Hutchinson, J.M.; Montserrat, S. Vitrification and devitrification during the non-isothermal cure of a thermoset. A TOPEM Study. "Journal of thermal analysis and calorimetry", Març 2010, vol. 99, núm. 3, p. 925-929. 
URIhttp://hdl.handle.net/2117/10298
DOI10.1007/s10973-009-0601-7
ISSN1388-6150
Publisher versionhttp://www.springerlink.com/content/102948/?k=Fraga+I&sortorder=asc&v=condensed&cb=2010&ce=2019
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  • TERFIQ - Grup de Termodinàmica i Fisico-Química - Articles de revista [61]
  • Departament de Màquines i Motors Tèrmics - Articles de revista [420]
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